Chapter 1Introduction of Experimental
Organic Chemistry1
11Basic Rules for the Organic
Chemistry Lab1
12Common Lab Equipment and
Apparatus2
13General Lab Safety7
14Disposal of Lab Waste9
15Common Organic Solvents9
16Experimental Preview Record and
Laboratory Report13
17Chemical Literature14
Reference15
Chapter 2Basic Experimental
Techniques17
21Heating and Cooling17
22Drying and Drying Agent17
23Filtration19
24Solvent Extraction and Solution
Washing21
25The Purification and Separation of
Liquid Organic Substances24
26The Purification and Separation of
Solid Organic Substances32
27Chromatographic Techniques38
28The Determination of the Physical Constant
of Organic Compound47
Chapter 3Comprehensive Experiment56
Part 1Synthesis56
31Synthesis of Cyclohexene56
32Synthesis of Ethyl Bromide57
33Synthesis of 2chlorobutane
(secbutyl chloride)59
34Synthesis of diethyl ether61
35Synthesis of Phenetole
(ethyl phenolate)62
36Synthesis of Benzoic Acid and
Benzyl Alcohol63
37Synthesis of Acetophenone65
38Synthesis of Benzophenone (Friedel
Crafts acylation method)67
39Synthesis of Cyclohexanone69
310Synthesis of Adipic Acid71
311Synthesis of Benzoic Acid73
312Synthesis of Cinnamic Acid74
313Synthesis of Ethyl Acetate76
314Synthesis of Isoamyl Acetate
(banana oil)78
315Synthesis of Acetylsalicylic
Acid (aspirin)79
316Synthesis of Methyl Salicylate
(oil of wintergreen)81
317Synthesis of Ethyl Acetoacetate83
318Synthesis of Acetanilide84
319Synthesis of ptoluidine86
320Synthesis of Anthranilic Acid
(2aminobenzoic acid)88
321Synthesis of Phenoxyacetic Acid90
322Synthesis of Methyl Orange92
323Synthesis of Benzocaine94
324Synthesis of Nacetylptoluidine96
325Synthesis of Benzoin96
326Synthesis of 2Nitroresorcinol98
327Synthesis of Quinoline100
328Synthesis of Nikethamide103
329The Reduction of Camphor104
330Synthesis of 3(2,5xylyloxyl)
Propyl Chloride and Monitoration of
Reaction Process106
Part 2Extraction and Separation107
331The Recrystallization of Benzoic
Acid107
332Extraction and Purification of
Nicotine109
333Isolation of Caffeine From
Tea Leave110
334Isolation of Effective Components
from the Citrus112
335Isolation of Benberine from Coptis
chinensis Franch114
336Paper Chromatography of Amino
Acid115
337Paper Electrophoresis of Amino
Acid117
338Separation of Green Leaf Pigments
by TLC119
Chapter 4Appendix121
41Experiments from the Literature121
42List of the Elements with Their
Symbols and Atomic Masses123
43Main Families of Organic
Compounds126
44Boling Point and Density of Some
Common Organic Reagents126
第1章有机化学实验基础知识127
11有机化学实验的基本规则127
12常用的玻璃仪器和实验装置127
13有机化学实验的安全知识129
14有机化学实验废物的处置130
15常用有机溶剂及纯化130
16实验预习记录和实验报告134
17有机化学的文献资料134
第2章有机化学实验基本操作136
21加热和冷却136
22干燥与干燥剂136
23过滤137
24萃取和洗涤139
25液体有机化合物的分离与纯化142
26固体有机化合物的提纯147
27色谱法151
28有机化合物物理常数的测定156
第3章综合实验163
第一部分制备163
31环己烯的制备163
32溴乙烷的制备164
332氯丁烷的制备165
34乙醚的制备166
35苯乙醚的制备167
36苯甲醇和苯甲酸的制备168
37苯乙酮的制备169
38二苯甲酮（酰基化法）的制备171
39环己酮的制备172
310己二酸的制备173
311苯甲酸的制备175
312肉桂酸的制备176
313乙酸乙酯的制备177
314乙酸异戊酯的制备（香蕉油）178
315乙酰水杨酸的制备（阿司匹林）180
316水杨酸甲酯的制备（冬青油）181
317乙酰乙酸乙酯的制备182
318乙酰苯胺的制备183
319对甲苯胺的合成184
320邻氨基苯甲酸的合成185
321苯氧乙酸的制备187
322甲基橙的制备189
323苯佐卡因的制备190
324对甲基N乙酰苯胺的合成192
325安息香的合成192
3262硝基雷琐酚的制备194
327喹啉的制备195
328尼可刹米的制备197
329樟脑的还原反应199
330降血脂药吉非贝齐中间体3（2，5二
甲基苯氧基）1氯丙烷的制备200
第二部分提取、分离与鉴定201
331苯甲酸的提纯201
332烟碱的提取与鉴定202
333从茶叶中提取咖啡因203
334橘皮中有效成分的提取、分离
与鉴定205
335黄连中黄连素的提取及鉴定206
336纸色谱分离鉴定氨基酸208
337纸上电泳分离鉴定氨基酸209
338薄层色谱法分离叶绿素210
参考文献212