- 高等教育出版社
- 9787040527124
- 1版
- 283626
- 46250991-0
- 平装
- 16开
- 2019-09
- 440
- 320
- 理学
- 化学
- 医学检验、药学类
- 本科
本书根据中国药科大学“双一流”建设和化学基础课程教学改革的需要编写，采用中英双语对照形式，注重对学生化学实验基本知识、实验操作技能的掌握，以及实验研究方法的启蒙与初步训练。
全书分为“基本要求与实验室规则”“实验基本操作与技能”“实验数据的处理”“实验部分”和附录。实验部分结合了药学相关内容，包括无机制备、无机定性分析、化学定量分析、化学常数测定，既可独立开设，也可以对其中的一些实验稍加整合，作为系列实验进行。附录部分除了常用数据表，还有药典中常见的无机离子鉴别。
本书可作为高等学校药学类专业本科生的基础化学实验课程教材，也可供医学、食品及化学化工等专业学生和社会学习者参考。
前辅文
Part 1 Laboratory General Information
1.1 Learning Objectives of the Course
1.2 General Guidelines
1.3 Honor Principle
1.4 General Safety Rules
Part 2 General Equipment and Lab Techniques
2.1 General Equipment
2.2 Cleaning Laboratory Glassware
2.3 Digital Balance and Weighing
2.4 Separation of Solids from Liquids
2.5 Heating
2.6 Measuring and Delivering Liquid
2.7 pH Meter and pH Measurement
2.8 Notebooks
2.9 Analysis of Data and Presentation of Results
Part 3 Quantitative Treatment of Data
3.1 Precision of Instrument Readings and Other Raw Data
3.2 Absolute and Relative Uncertainty
3.3 Accuracy and Precision
3.4 Error
3.5 Average Deviation and Standard Deviation
3.6 Significant Figure
3.7 Statistics Applied to Small Data Sets
3.8 Propagation of Indeterminate Errors
Part 4 Experiments
Experiment 1 Checking and Cleaning Equipment
Experiment 2 Weighing Exercise and Preparing Solutions
Experiment 3 Determination of the Water of Crystallization in Barium Chloride
Experiment 4 Preparation of Ferrous Ammonium Sulfate Hexahydrate
Experiment 5 Preparation of Zinc Gluconate
Experiment 6 Preparation of Medicinal Sodium Chloride and Examination of Impurities Limitation
Experiment 7 Synthesis of Potassium Aluminum Sulfate (Alum)
Experiment 8 Qualitative Analysis of Cations (1)
Experiment 9 Qualitative Analysis of Cations (2)
Experiment 10 Designing Scheme for Qualitative Analysis of Cations
Experiment 11 Calibration of Volumetric Glassware
Experiment 12 Preparation and Standardization of a Standard Sodium Hydroxide Solution
Experiment 13 Preparation and Standardization of a Standard solution of Hydrochloric Acid
Experiment 14 Determination of Aspirin (acetylsalicylic acid) using Back Titration
Experiment 15 Determination of Medicinal Zinc Oxide
Experiment 16 Determination of Borax for Pharmaceutical Use
Experiment 17 Determination of a Mixed Base
Experiment 18 Preparation and Standardization of EDTA Solution
Experiment 19 Content Assay of Zinc In Medicinal Zinc Gluconate
Experiment 20 Determination of Water Hardness
Experiment 21 Determination of Aluminium Potassium Sulfate in Alum
Experiment 22 Precipitation Titration: Determination of Chloride by Mohr Method
Experiment 23 Preparation and Standardization of Perchloric Acid in Non-aqueous Solvent
Experiment 24 Determination of Sodium Salicylate in Non-aqueous Solvent
Experiment 25 Preparation and Standardization of Potassium Permanganate Solution
Experiment 26 Assay of Ferrous Ammonium Sulfate
Experiment 27 Determination of Medical Hydrogen Peroxide
Experiment 28 Preparation and Standardization of 0.05 molL−1 Iodine Solution
Experiment 29 Iodimetric Titration of Ascorbic Acid in Vitamin C Tablets
Experiment 30 Determination of Dissociation Constant of Weak Acid
Experiment 31 Buffer Action and Buffer Solution
Experiment 32 Determining Coordination Number of [Ag(NH3)n]+ Complex
Experiment 33 Determination of Reaction Rate and Activation Energy
Experiment 34 Determination of Ksp of Silver Acetate
Part 5 Appendix
5.1 Identification Tests of Common Inorganic Ions
5.2 Ionization Constants of Inorganic Acids and Bases
5.3 Common Primary Standards
5.4 Common pH Buffer Solution
5.5 Common Indicator
